由于氨基存在,挥发性胺类溶剂与色谱柱以及样品流路活性位点相互作用,造成的宽峰和拖尾。
胺通常是在水、酒精或氨水的环境下进行分析的,基质苛刻,色谱柱耐受性易下降。
挥发性胺类沸点较低,相对保留较较弱。
浩瀚色谱(山东)应用技术开发有限公司,研制的HH-AMB胺分析专用柱,测定一甲胺,二甲胺,三甲胺,柱效高,分离好,分析时间短,应用在安捷伦,岛津,赛默飞,瓦里安,布鲁克,PE,磐诺,天瑞,天美,科创,川仪等仪器上,定量准确。
名称:胺分析专用柱B
型号:HH-AM
规格:3m*1/8,60-80目
最高使用温度:120°C
编号:20241025001
应用:分离空气,氨,一甲胺,二甲胺,三甲胺,甲醇,水分; 柱效高,分离好,峰型对称,结果满意。
GB/T 30303-2013 工业用甲胺和甲胺水溶液试验方法
HG/T 2971-1999 工业甲胺水溶液试验方法
用于分析由甲醇连续气相催化氨化法生产的二甲胺配制成的40%水溶液
Due to the presence of amino groups, volatile amine solvents interact with the chromatographic column and active sites in the sample flow path, resulting in broad peaks and tails.
Amines are usually analyzed in environments such as water, alcohol, or ammonia solution, with harsh matrices and decreased column tolerance.
Volatile amines have lower boiling points and relatively weaker retention.
Haohan Chromatography (Shandong) Application Technology Development Co., Ltd. has developed a HH-AMB amine analysis column specifically designed for the determination of dimethylamine, dimethylamine, and trimethylamine. The column has high efficiency, good separation, and short analysis time. It has been applied to Agilent, Shimadzu, Thermo Fisher Scientific, Varian, Bruker, PE, Panno, Tianrui, Tianmei, Kechuang, Chuanyi and other instruments with accurate quantification.
Name: Amine Analysis Column B
Model: HH-AM
Specification: 3m * 1/8, 60-80 mesh
Maximum operating temperature: 120 ° C
Number: 20241025001
Application: Separation of air, ammonia, methylamine, dimethylamine, trimethylamine, methanol, and moisture; High column efficiency, good separation, symmetrical peak shape, satisfactory results.
GB/T 30303-2013 Test Methods for Industrial Methylamine and Methylamine Water Solutions
HG/T 2971-1999 Test Method for Industrial Methylamine Water Solution
Used for analyzing a 40% aqueous solution prepared from dimethylamine produced by continuous gas-phase catalytic amination of methanol