本文件规定了采用顶空气相色谱法测定含氢硅油中含氢量（Si-H 中 H 的质量分数）的方法。 本文件适用于高含氢硅油、低含氢硅油、端含氢硅油中含氢量的检测。

　　浩瀚色谱（山东）应用技术开发有限公司，采用气相色谱法对含氢硅油和聚醚硅油中的含氢量进行了测定。其原理是利用Si-H键与NaOH溶液反应产生氢气,通过准确测定生成氢气的体积，算出含氢量,并与化学法进行了对比,结果表明两者间相对偏差均小于3.3%,取得了满意的效果。

　　名称:5Å分子筛填充柱

　　规格:6FT*1/8，60-80Mesh

　　最高使用温度:320°C

　　应用:含氢硅油中含氢量的测定 顶空气相色谱

　　This document specifies the method for determining the hydrogen content (mass fraction of H in Si-H) in hydrogen containing silicone oil using headspace gas chromatography. This document is applicable for the detection of hydrogen content in high hydrogen silicone oil, low hydrogen silicone oil, and end hydrogen silicone oil.

　　Haohan Chromatography (Shandong) Application Technology Development Co., Ltd. used gas chromatography to determine the hydrogen content in hydrogen containing silicone oil and polyether silicone oil. The principle is to use Si-H bonds to react with NaOH solution to generate hydrogen gas. By accurately measuring the volume of hydrogen gas generated, the hydrogen content is calculated and compared with chemical methods. The results show that the relative deviation between the two is less than 3.3%, achieving satisfactory results.

　　Name: 5 Å Molecular Sieve Filled Column

　　Specification: 6FT * 1/8, 60-80 Mesh

　　Maximum operating temperature: 320 ° C

　　Application: Determination of hydrogen content in hydrogen containing silicone oil by headspace gas chromatography