城市燃气中氨含量的分析方法上,现在执行的是GB12210-90标准.其中取样时燃气流速规定在0.25~0.5L/min,并要求吸收的氨量控制在 2~30mg范围内.当燃气中的氨含量在50mg/m3平均取样 速度为0.38L/min,平均吸收的氨量为16mg,则需取0.32m3煤气.取样时间为320/0.38=842min,合14个多小时.由此可见, 取样需要的时间很长,而当煤气中氨含量较低时(经常有<20mg/m3),则需要采样时间更长.
浩瀚色谱(山东)应用技术开发有限公司,研制的HH-NH3.H2O氨专用色谱固定相,装柱测试高纯氨,柱效高,峰型对称,适用于工业氨水,高纯氨气,燃料氢中微量氨,合成氨,焦炉煤气中氨气,燃气在氨气等的分析测定,实验结果满意。
气相色谱固定相 NH3.H2O
粒度:80-100目 25g
温度:200°C
编号:20240202002
配套于安捷伦,岛津,赛默飞,瓦里安,布鲁克,pE等。
The analysis method for ammonia content in urban gas currently follows the GB12210-90 standard. The gas flow rate during sampling is specified to be 0.25-0.5L/min, and the absorbed ammonia amount is required to be controlled within the range of 2-30mg. When the ammonia content in the gas is 50mg/m3, the average sampling speed is 0.38L/min, and the average absorbed ammonia amount is 16mg, then 0.32m3 of gas needs to be taken. The sampling time is 320/0.38=842min, which is more than 14 hours. It can be seen that the sampling time is very long, When the ammonia content in the gas is low (often<20mg/m3), a longer sampling time is required
The HH-NH3.H2O ammonia specific chromatographic stationary phase developed by Haohan Chromatography (Shandong) Application Technology Development Co., Ltd. has been tested for high-purity ammonia with high column efficiency and symmetrical peak shape. It is suitable for the analysis and determination of trace ammonia in industrial ammonia water, high-purity ammonia gas, fuel hydrogen, synthetic ammonia, ammonia in coke oven gas, and ammonia in gas. The experimental results are satisfactory.
Gas chromatography stationary phase NH3. H2O
Particle size: 80-100 mesh 25g
Temperature: 200 ° C
Number: 20240202002
Supported by Agilent, Shimadzu, Thermo Fisher, Varian, Brooke, pE, etc.